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Adsorption of methylene blue by magnetized achiote (Bixa orellana) pericarp ash: Effect of pH and kinetics
Arellano, Jeramay, M. (Davao del Sur State College, 2024-06)
Wastewater management has long been a significant issue for society. In the Philippines, achiote pericarp is often considered an agricultural waste. It is typically left in open fields or burned in the open air near the trees where they are harvested. This study explores the potential use of this waste material (achiote pericarp ash, APA) in removing dye from liquid solutions. To improve the adsorption capacity of APA, it is necessary to incorporate Fe3O4 into it. This will enhance its ability to effectively adsorb Methylene blue solution. To address this, APA had been impregnated with Fe3O4 nanoparticles to produce magnetized APA (MAPA). The APA used in this study was sourced from the farmlands of J. P. Laurel Malungon, Sarangani, Philippines. An adsorption experiment was thoroughly conducted, investigating the effects of pH and kinetic changes. The MB adsorption process was found to fit with a pseudo-quadratic model, with maximum adsorption observed at pH 10. The identification of functional groups presents before and after magnetization was conducted using Fourier transform infrared spectroscopy (FTIR). Among theme were -OH (intramolecular H-bond), O=OH (phosphorus oxoacid), -CO-CH3 (ketone), -OH (primary alcohol), and -SiCl3 (silicon compounds). These findings encourage farmers to reuse agricultural waste as a valuable product. Future related research could investigate the use of a different dye color or another type of biomass. Ultimately, this investigation provides significant knowledge about the potential role of agricultural by-products for wastewater treatment processes.
Conductive effect of ferric chloride (FeCl₃) on carbonized Chloris barbata Sw. stem via activation-carbonization-pyrolysis method
Retiza, Debie T. (Davao del Sur State College, 2024-05)
This study was conducted to determine the conductive effect of ferric chloride (FeCl₃) on carbonized Chloris barbata sw. stem via the activation-carbonization-pyrolysis method. The study was accomplished utilizing a Completely Randomized Design, which comprised five (5) treatments and three (3) replications. The activated carbon produced was made using C. barbata stem and ferric chloride (FeCl₃) at different molar concentrations. Control -no FeCl₃(T1), 1 molar concentration (T5). The study was carried out to determine the electrical conductivity, surface characteristics in terms of pore and elemental composition, surface area, and the cost analysis of the activated carbon. The data were analyzed using One-Way ANOVA of variance at 1% and 5% significance levels, Scanning Electron Microscope (SEM), Energy Disperse X-ray Spectroscopy (EDX), Brunauer-Emmett-Teller (BET), and Fourier Infrared Spectroscopy (FTIR). The results revealed that the electrical conductivity of all treatments was shown to be statistically highly significant. According to the findings, T5 (4 M) registered the highest electrical conductivity at 2677.06 x 10^-6 μS/m. It was also found to display micropore structure and various organic and inorganic functionalities, register relatively low surface area, and more acceptable production cost per unit mass.